PREPARATION AND ANALYSIS OF SCHIFF BASE DERIVED FROM ANILINE AND ACETYLACETONE AND ITS NI(II) COMPLEX

Student: Juwairiyya Ibrahim
Supervisor: Mrs Bashariyya Abdullahi Lawal
HOD: Prof Umar Sani
Department of Chemistry
Physical Sciences
Bayero University, Kano, Kano State

Abstract

ABSTRACT A Schiff base derived from condensation reaction between Aniline and Acetylacetone was prepared and characterized, along with Ni(II) complex. The preparation involved the reaction of Acetylacetone with Aniline in an ethanol solvent under reflux conditions. The resulting Schiff base was characterized using various spectroscopic technique, including IR spectroscopy. The presence of characteristic absorption bands in the IR spectrum confirmed the formation of the Schiff base, the Schiff base was complexed with Ni(II) chloride to form a metal complex, which was characterized using similar spectroscopic techniques. The characterization data provided valuable information about the structure and properties of both the Schiff base and its Ni(II) complex.

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